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By W. Albert, Jr. Noyes

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Unfortunately, the details of the algorithms for calculating the structural parameters have not been described in detail. Due to the lattice rigidity, some of the unreacted groups cannot find their reaction partners and remain unreacted ; this is called the topological limit of the reaction. A few of these groups can also form monocycles (cf. 4 of Ref. 14) ). This topological limit was confirmed by some experiments, some other authors claim, however, that they can reach 100% reaction. An accurate determination of the few unreacted groups in the rigid structure is, however, not an easy task.

Much more data are needed, however. The position of the gel point on the conversion scale is of primary interest in a branching process. The critical conversion for the diepoxide-diamine systems with groups of independent reactivity depends on the initial molar ratio of amino to epoxy-amine systems22), and they agree within experimental error with the predicthe amino group characterized by Q. Figure 9 shows the theoretical predictions for various Q and the experimental points for the system DGEBA-hexamethylenediamine (HMDA).

13. Dependence of the reduced modulus Gr (mol/cm3) and of the trapped entanglement contribution A (mol/cm3) on rA for the cured DGEBA-PGE-DDM systems 17'18'. o measurements in the , theoretical dependence for the dry state, 0 samples swollen in dimethylformamide; a theoretical dependence using e = 8 x I0~4 mol/cm3 value of front factor A indicated, b In conclusion, it can be said that the theory can well describe the development of the gel structure. The correlation between the equilibrium modulus and sol fraction is very good 18) so that the sol fraction can alternatively be used for determination of the concentration of EANC's if an accurate and precise determination of conversion meets with difficulties.

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Advances in Photochemistry [Vol 1] by W. Albert, Jr. Noyes

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